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Beilstein J. Org. Chem. 2014, 10, 902–909, doi:10.3762/bjoc.10.88
Graphical Abstract
Scheme 1: Synthesis of Z-configurated model compounds 3a/b from E-benzaldoxime and acrylates 2a/b.
Figure 1: 1H NMR spectra of 3a (300 MHz, DMSO-d6).
Scheme 2: Proposed molecular interactions of nitron 3a and dimethyl itaconate (4).
Scheme 3: 1,3-Dipolaric cycloaddition of nitrones 3a/b with dimethyl itaconate (4).
Scheme 4: Synthetic route to bio-based dinitrones derived from isosorbide.
Scheme 5: Synthesis of poly(isosorbide itaconate -co- succinate) 13 from isosorbide (6), itaconic acid (11) a...
Figure 2: Oscillation measurements during thermal cross-linking of unsaturated polyester 13 with dinitrones 1...